Quality Assurance of Selective Laser Melting Applications

By Thomas Gruenberger

Key differentiation criteria for Additive Manufacturing (AM) technologies are freedom of design, cost advantage, customization, and time to market.

Direct metal laser sintering (DMLS) AM technology is ideal for serial production for industries like aerospace.

Setting up a process means mapping the input parameters (e.g. machine and process parameters and part geometry) to output parameters (part properties like density, tightness, surface quality). An in-situ nondestructive measurement of part properties like density is not possible, so indirect measurements have to be performed. Information from the process – process emissions, melt pool size, melt pool dynamics, and temperature distribution – can be used for this indirect measurement enabling the user to find a correlation between features of these measurements and the resulting part properties. Additionally, a shorter process development time can be achieved by avoiding destructive tests during development learning reading the extracted features (see Fig. 1).

Fig. 1: Quality inspection – the challenge

As mentioned above, several pieces of information from the process can be used for the detection of irregularities, so different sensor technologies can be used. Consider a manual in-situ inspection of the process, where the user looks at the visible process emissions in the process chamber. Differences in brightness, size, color, and number of sparkles can be detected with the human eye. This can be automated using photodiode based meltpool monitoring systems like the plasmo fast process observer, a hardware developed by plasmo with up to 4 channels at sampling rates up to 300kHz.

So the system measures the brightness of the process emissions over time (blue curve in Fig. 2), using CAD data, the data can be mapped easily to an image of brightness of process emissions over the building platform (see Fig. 2 right plot), layer for layer, in pseudo color representation.

Fig. 2: Feature map of the building process

Running an OK process gives the baseline of the feature, provoking process irregularities yields in a change of the feature, enabling the user to set limits for the feature according to its quality needs. A pseudo color representation of a map of process irregularities can be calculated, giving the user an easy way to understand visualization and therefore, fast feedback about the quality of the process. As a note, black means no process irregularities and yellow means 100 percent of process irregularities in the given pixel in Fig. 3.

Fig. 3: Map of process irregularities

The fully automated measurement system enables a 100 percent inspection of the building process. The high sampling rate (ca. 10,000 times fa

ster compared to the human eye) enables the system not only to calculate features like signal height but the additional analysis in time, frequency and time scale domain can be performed, too. Three (3) different algorithms (features) are calculated by the system and each algorithm can be parametrized according to the quality needs for every exposure type used in the layer.

These algorithms are easy to explain. Based on physics, they correspond directly to process different phenomena.

  • Absolute limits: Influences in the size and form of the cross section of one exposure like focal position, laser power and welding speed
  • Signal dynamics: Noisy processes or less process dynamics like pollution, protective gas flow and lack of fusion
  • Short time fluctuations: Short changes in the signal caused by e.g. ejects and pollution

In cooperation with EOS, the described system was integrated with their machines. A typical layout is shown in Fig. 4.

Fig. 4: System layout – EOSTATE Meltpool

As shown in Fig. 4, two total photodiodes are used an onAxis diode measuring the process emissions at the interaction zone of the laser beam and powder and an offAxis diode giving an overview of process emissions about the complete building platform.

A heuristic model is used for setting up the system; therefore, input parameters like process parameters (laser power, scanning speed, gas flow, …) and malfunctions like loss of laser power, and material quality are varied for different building jobs. The output parameters are part properties (porosity, surface roughness, …), process emissions (brightness, temporal behavior, spectral properties, …) and undesired effects like overheating, warpage and lack of fusion. Based on this data set the system can be parametrized to fulfill the quality needs of the customer.

Fig. 5 shows a provoked malfunction, missing powder choosing a too low dosing factor of powder, the irregularities (here red in Fig. 5) can be easily detected.

Fig. 5: Example missing powder, left image of powder bed, right calculated irregularities after exposure

Fig. 6 shows a phenomena process flipping provoked by changing the focal position, the irregularities (red in Fig. 6) can be detected successfully for the complete parts and also the embedded parts (letter F).

Fig. 6: Example process flipping, left image of building platform after complete build, right calculated irregularities

Successful detection of additional phenomena has been shown:

  • Overhanging parts
  • Dust/particles
  • Part overlap
  • Balling / humping
  • SLI pores (simulated porosity)
  • To be continued.

The presented diode based meltpool monitoring system enables the fully automated detection of process phenomena (see Fig. 7) which directly corresponds to part properties.

Fig. 7: Example stable and unstable process, top image of process emissions, middle measured brightness, bottom windowed FFT analysis

Easily understandable algorithms based on physics are applied and can be parametrized by the user according to its needs. A heuristic model for setting up limits was presented and examples of detectable process phenomena are given. The system is part of an integrated quality inspection portfolio at EOS including EOSTATE powderbed and EOSTATE system monitoring.

Further investigations in detectable process phenomena and self-healing effects of defects will be completed. Additional work is in progress in the field of statistical data processing, so information (see Fig. 8, e.g. trends, …) is extracted from data visualized in dashboards enabling the user to perform statistical process control (SPC) at one machine up to different machines at different locations worldwide.

Fig. 8: Statistical process control

About plasmo 

Headquartered in Vienna, Austria, plasmo is an innovative, globally operating technology company for automated quality assurance systems in manufacturing industries. Established in 2003, plasmo leads the way in the real-time quality control of joining processes. The extensive portfolio in the field of quality assurance includes laser power measurement, the monitoring of welding processes, geometric shapes and surfaces, tailor-made solutions in the field of industrial image processing, analysis software as well as an extensive range of services.

With over 700 plasmo systems in operation worldwide, the growing list of clients includes ABB, Benteler, BorgWarner, Faurecia, INA, SMS Siemag, Hettich, JCI, Magna and Valeo to Webasto, and numerous automobile manufacturers such as Audi, BMW, Daimler, Ford, GM, PSA, Suzuki, Volvo as well as various international steel manufacturers. www.plasmo-us.com

© 2017 Dr. Thomas Grünberger, plasmo Industrietechnik GmbH, Vienna

 

Laser Additive Manufacturing for Aerospace Prototypes

By: Agnes Klucha

Pratt & Whitney

Aerospace prototyping is a way to realize the vision of freeform fabricated metal additive manufactured parts on aerospace production engines, gain acceptance for additive manufacturing and change perceptions of what is possible.  The freeform fabrication of laser additive manufactured metal parts is of prime interest in aerospace prototyping since a functional prototype can be delivered quickly to demonstrate and validate concept designs. Continue reading

Laser Sintering of Silver Nanoparticles

By: Petri Laakso

INTRODUCTION

Roll-to-roll printing itself is not always sufficient for the production of printed electronics components

and systems. Drying and sintering are the bottleneck processes in metal particle based conductor printing. Lasers show high potential for the curing process, especially in the case of nanoparticulate inks. This is due to fact that the typical sintering temperatures for nanoparticles (100–300°C) are only a fraction of the macroscopic melting point of the corresponding materials. This allows paper or plastic substrates to be used.

MATERIALS AND METHODS

Base material in sintering was polyimide. Laserline fiber coupled diode laser with scanhead was used for sintering.

SINTERING RESULTS

The sintering of printed nanoparticle structures using laser treatment has been investigated at VTT. Laser sintering can be utilised in the manufacturing of printed conductor structures such as antennas, circuits and sensors [1, 2]. A drop-on demand printer was used to print patterns with metal-organic silver nanoparticles on a flexible polyimide substrate. Laser sintering was done with a 940 nm CW fibre-coupled diode laser. The process was optimised using different scanning speeds, laser power levels, line separation and repetition rounds. In sintering tests, three different line thicknesses were printed to gauge the effect of line width. Sintering tests were done with Ink 1 using the hatch technique. The laser speed was 1000 mm/s and the line-to-line distance was 0.2 mm. The beam size was 1 mm in diameter. After a series of pre-tests, the optimal range of average power were estimated to be between 20–50 W. Table 1 shows the effect of average power and conductor width on sheet resistance.

Table 1. Sheet resistance values with different average powers on ink 1 with different conductor widths.

50 W 40 W 30 W 20 W
100 µm 0.16 0.18 0.29 0.52
200 µm 0.17 0.27 0.31 0.59
350 µm 0.16 0.19 0.28 0.38

SUMMARY

Laser sintering of nanoparticle inks seems to be promising curing technique for R2R sintering. Especially in cases

where only part of the substrate need to be cured, laser has the potential for reaching a high processing speed.

Additionally it can allow low-cost low melting point substrates to be used since heating is well-targeted to inks.

Choosing the right ink for the process and keeping the substrate clean are key factors for successful operation.

Sheet resistance values only slightly exceed the values obtained by heat sintering. This result was obtained in preliminary test and can be further optimised.

BUSINESS POTENTIAL

Laser sintering has a high potential for curing metal particle inks on flexible substrates. It offers a fast processing speed and low temperature processing, and therefore, it often represents an improvement over oven sintering.

REFERENCES

[1] Khan, A.; Rasmussen, N.; Marinov.; Svenson, O.: Laser

Sintering of Nanomaterial on Polymer Substrates.

In: journal of Microelectronics and electronic Packaging

(2008)5, 77-86

[2] Ko S.; Pan H.; Grigoropoulos C.; Luscombe C.; Frechet

J.; Poulikakos D.: All-inkjet-printed fl exible

electronics fabrication on a polymer substrate by

low-temperature high-resolution selective laser sintering

of metal nanoparticles, Nanotechnology 18

(2007) 345202.

ACKNOWLEDGEMENTS

Laser sintering work was done in a TEKES funded PESEP -project. The ink jet printing for laser sintering trials was done in this project by Eerik Halonen from the Tampere University of Technology.

The above brief overview was extracted from its original abstract and paper presented at The International Congress on Applications of Lasers & Electro-Optics (ICALEO) in Orlando, FL. To order a copy of the complete proceedings from this conference click here

Effect of Substrate on Temperature Field in Selective Laser Sintering of Metal Powders

By: Shen Xianfeng

Selective Laser Sintering (SLS) of metal powders, namely Direct Metal Laser Sintering (DMLS) is an emerging Rapid Prototyping and Manufacturing (RPM) technology which can be used to produce three-dimensional metal parts directly from a CAD model by the selective laser sintering (SLS) of successive layers of metallic or pre-alloyed powders. SLS of metal powders is becoming a significant trend of Direct Manufacture (DM) for the unique advantage in direct manufacturing of metal parts and eliminating the expensively time-consuming pre- and post-processing steps, compared to indirect laser sintering or other conventional processes. In the laser sintering process of metal powder, the substrate plays an important role in DMLS. As a matter of fact, the substrates are commonly used for avoiding the balling effect in powder melting and dislocation of sintered part. So the issue of the substrate role in the process is becoming one of the research focuses. Continue reading