A Legacy in Lasers

Professor Steen having been awarded the AILU Award in 2005, recognising his outstanding contribution to the industrial use of lasers in the UK

As featured in Laser Systems Europe Autumn 2019.

The LIA has introduced a set of annual awards dedicated to Professor William Maxwell Steen, a veteran and pioneer of laser technology.

This year the Laser Institute (LIA) announced a new set of awards that it plans to confer annually to user organisations that demonstrate significant innovation in the use of lasers for advanced materials processing. Finalists and recipients of the awards will present their innovations at the International Congress on Applications of Lasers & Electro-Optics (ICALEO) on 7-10 October.

The awards will be conferred across each of the following industries: aerospace; automotive; medical devices; microelectronics; specialised manufacturing and services; research and development; life sciences; defense; academic and public sector.

They are dedicated to Professor William Maxwell Steen, a pioneer of laser materials processing research who is commonly referred to as ‘the father of laser materials processing’ in the industrial laser community.

Steen, in addition to founding the world’s first university-based research group in laser material processing at Imperial College London in 1968, can be accredited with the invention of laser chemical vapour deposition, laser arc hybrid welding, and with his research group, the development of blown powder laser cladding and laser direct casting – processes which formed the foundation of laser additive manufacturing for metallic materials, more commonly known today as 3D printing.

Emma Johnston being presented with the AILU Young Engineer’s Prize by John Bishop (left) and Professor Steen, who was Emma’s PhD supervisor at Liverpool University and AILU president at the time

He also co-founded the Association of Industrial Laser Users (AILU) in 1995 and served as its president for the first eight years. In addition, in 1997 Steen was the first European to be awarded the Arthur Schawlow Award by LIA, and at ICALEO 2008 there was a tribute session to his lifetime achievements. He has a laboratory named after him at the University of Vigo, Spain, and has received a medal from Pelacky University in Oloumouc, Czech Republic, for his pioneering work on lasers.

Steen’s textbook Laser Material Processing – the fourth edition of which was published in 2010 – has for years been a vital source of information for students, researchers and engineers learning laser material processing. Many of Steen’s ex-students (and even their ex-students) now either run their own business, teach, or make money from laser material processing.

On hearing the announcement of the new award, Laser Systems Europe approached Steen to find out more about his many experiences exploring the realm of laser technology.

When did you first begin working in laser technology?

In 1964 I was appointed lecturer at Imperial College London in process metallurgy. I became interested in metal extraction by volatile compounds, such as chlorides, and this led to trying to make patterns by depositing metal from volatile compounds, such as nickel carbonyl. I realized that the pattern created using shaped jets on hot plates was very blurred, and thus needed to make a shaped hot spot. I bought a glass tube with mirror mounts from Ealing Scientific, built my own power supply and I had a very unstable 5W CO2 laser on which I invented the process of laser chemical vapour deposition (LCVD), which worked but obviously needed more power.

In working this up I won a contract for the first industrial fast axial flow 2kW CO2 laser from BOC developed by The Welding Institute (TWI). That gave me the most powerful university-based laser in the UK. Students and contracts flowed from this with the wide-open space for research using this entirely new form of industrial energy.

As a pioneer of laser technology for industrial materials processing, how has industry’s view of laser technology changed?

The very early years were dominated by numerous small start-up laser companies wishing to sell their lasers and compete to find useful applications at sensible prices, this was the main challenge – a solution looking for a problem. Cutting and welding were the only applications at that time with some curious results.

Martin Adams, at TWI, was publishing cutting figures significantly better than everyone else, but because of the atmosphere of competition, this was explained as commercial optimism. Later we came to realise he was able to cut nearly twice as fast as others because TWI had not the space for the cutting table other than in line with the laser, and the beam polarisation favoured his layout as opposed to those with transverse tables; a feature of optical energy not fully understood in those exciting times. There were many more surprises to be found as we explored this new form of energy!

For the next 20 years or so, the reliability and ease of maintenance of lasers improved, with most industries keeping a watching brief on what was going on. I felt at the time I could go to any company and sell the idea of a laser application as a result of this interest.

In the 1990s the fibre laser arrived on the scene and the game changed. The fibre laser was smaller, required less cooling, had no alignment problems and a superb loworder mode beam. To some extent it was like a dream come true.

Today, reliability and quality are taken for granted, and the only thing holding the laser back now is cost, which is rapidly coming down as more units are required. It used to be good to see the look of awe on people’s faces when you said you worked with lasers, now it is not really regarded as unusual. In summary, the opinion of industrialists today is that the laser has arrived, and they are learning to live and work with it.

Are there any particular applications of laser technology you’ve enjoyed watching develop since your retirement in 1998?

There are many applications I have enjoyed working on, but additive manufacturing comes immediately to mind as something special – a game changer in the thinking of how to make things. In the 1980s Rolls Royce asked us to blow powder into the laser beam and so we invented the laser cladding process. It worked

Professor Steen being presented with an Honorary Fellowship to the Institution of Mechanical Engineers by the institute’s president Carolyn Griffiths

so well it became similar to writing with metal, then one day one of my students, Mark McLean, repeatedly overlaid a clad line and produced a wall. One look at that wall, particularly after a metallurgical examination showed the columnar grains running up the wall instead of across the wall – as in a standard casting – showed that we had a serious new manufacturing process on our hands.

Mark went onto make a stainless-steel wine glass, and additive manufacturing was born. Students of mine over the world have now worked on this promising development.

I watch with both amazement and joy at the ingenuity of what is being done with additive manufacturing, and await the day that someone makes a hand-held device, either wire or powder-fed whereby the craft community can actually sculpt in reverse – building things up instead of chiselling material away. The precision is such that in the hands of a craftsman, stunning works of art would be created. If the price is right there would be a huge market for such equipment.

Are you satisfied with how university laser research groups around the world are interacting and collaborating?

There is quite a network of friends among my ex-students based at various institutes around the world who have a strong collaboration, while still remaining competitive, which is as it should be.

One of my main concerns is the lack of imagination at universities. It is obvious to me and others working with lasers that they are dealing with an unusual and highly flexible form of energy available in a uniquely controllable form which can be of almost unlimited power, from milliwatts to petawatts, deliverable in times ranging from continuous to femtoseconds or even less, over a huge range of wavelengths.

The applications of this energy range from material processing through to sensing, metrology, communications, medicine, fluorescence, interferometry, holography and x-rays. This is far more than electricity has to offer, and yet there are currently very few or no university departments dedicated to optical energy – amazing!

Could you give an example from you career where academia has interacted well with industry?

One of our most successful developments came from the work of Professor Lin Li – a past president of LIA and AILU now at Manchester University – who while exploring the possibility of sealing concrete by surface melting – for ease of cleaning, sterility etc – found that thermal cracking made this difficult.

In expanding the beam to try and avoid this he found that he could explosively remove the top centimetre of the surface in reasonably large lumps. Such a simple process was taken up by British Nuclear Fuels (BNFL) for scabbling the walls of radioactive tanks prior to decommissioning. Lin Li proved the process worked and BNFL developed it further at TWI and finally used it for real in their works.

This initiative of the LIA in instituting annual awards for the best developments coming from industry or universities should further enhance academia’s connectivity with industry, and it is very flattering that the LIA has named these awards after me!

Do you have any pearls of wisdom for those looking to start their own entrepreneurial laser journey?

It is certainly stimulating to watch my students set up a business. Those that succeed either need good financial backing and/or a great determination to win. For example, Dr John Powell started Laser Expertise in Nottingham with two friends, they were young, energetic and disciplined in work habits and finance. They spent within their budget by buying a second-hand laser and worked several years for very little return while they expanded the business of a laser job shop. John had a partner for finance, a partner for sales, and he himself had a talent for invention and much more. Together the three of them made a success of the company, which I believe now employs some 60 people.

So, if there is any pearl of wisdom, it is to have a belief in yourself and a determination to win, even when the going is tough. In the laser business the rewards can be great, with much excitement and potential novelty at any time.

 

A full version of this interview can be found online at www.lasersystemseurope.com

SOURCE: https://content.yudu.com/web/tzly/0A43q4s/LSEaut19/html/index.html?page=34&origin=reader

Goodbye Adhesives, Hello Thermal Direct Joining

Laser Pre-Treatment and the Future of Hybrid Materials

Interview by Liliana Caldero

Originally in LIA TODAY July/August 2019.

Throughout the world, scientists are rising to the challenge of developing new techniques to improve the eco-friendliness of products and production lines. Germany has been among the strongest supporters of the movement to be more environmentally responsible. Innovations resulting from this momentum may lead to more efficient manufacturing, which could ultimately cut costs without compromising quality. Hybrid materials are growing in importance in the search for strong, lightweight materials that produce fewer CO2 emissions. Dominic Woitun of the German-based Bosch is among the researchers investigating techniques for effective thermal direct joining of hybrid materials. Joining dissimilar materials such as metals and plastics can pose a challenge; this challenge is often solved with the use of adhesives or screws with sealants. Adhesives may work, but according to Woitun, they leave a larger carbon footprint. This is where thermal direct joining comes in. The process that Woitun is researching involves using laser ablation to shape macroscopic structures into a metal surface; the structures  are then penetrated  with a  molten polymer which enables mechanical fastening, for instance. After solidification, a strong joint is obtained, which replaces the need for an adhesive. The shapes, or geometries, created by the laser play an important role in the strength and reliability of the joint, so better understanding the relationship between these geometries and the resulting joint will help make this a viable alternative to adhesives. Woitun shared with LIA TODAY why he started researching the impact of laser geometries on thermal direct joining of hybrid materials, and why companies could consider this an answer to adhesives.

LIA: For some in our community, the term ‘thermal joining’ brings to mind laser welding of metals; for those who are new to the concept of thermal direct joining of hybrid materials, could you describe what this process can look like, step-by-step?

DW: Thermal direct joining is a joining technique for metals and polymers. The adhesive forces of a thermoplastic melt to metals is used to join both partners. No additional adhesive is needed. However, to achieve strong joints, some form of surface pretreatment is needed. Laser structuring is a promising approach.

The process steps to a finished part could look like this:

  1. Preparation: prior surface treatment (e.g. by laser ablation)
  2. Joining: Many different techniques are possible! The only premise is a somehow molten polymer in the joining interface that can penetrate the structure. This can be achieved, for example, by heating the metal part with some kind of heat source and then pressing it onto the plastic part. Or, in my case, by using injection molding and overflowing the metal part with molten polymer in the molding tool.
  3. Finishing: the molten polymer solidifies instantly and directly after joining the joint has almost its final strength

LIA: Tell us about what drove you to research thermal direct joining?

DW: In order to meet today’s requirements for weight reduction and thus emission reduction, hybrid components are becoming increasingly important. Especially in the context of electrification. One main challenge for the production readiness of hybrid composites is the joining technology. Currently, hybrid parts are often joined by adhesives or screws in combination with sealants. Therefore, the interfaces need to be handled with special care and must be cleaned before joining. After joining, the parts need a certain curing time before they can be further processed. When it comes to recycling, there is almost no way to separate the often used and recyclable thermoplastic material from the duroplastic adhesives. This makes the current solutions time-consuming and costly.

LIA: What are you researching right now and how does it help to solve these challenges?

DW: Direct joining of metals and polymers based on a laser-pretreatment bypasses these problems and produces strong and media tight joints directly after the joining process. However, the enormous variety of laser sources, in combination with their adjustable parameters, open up endless possibilities for structures on the metal surface. This often ends in time-consuming empirical studies to find the best settings for one specific use case. That’s why I’m investigating the influence of largely separated surface characteristics on the joint properties by generating well-defined structures on the metal surface by laser ablation. My aim is to find the best weighting and composition of surface characteristics to define the optimal structure for an application.

LIA: What benefits could companies gain from utilizing direct joining?

DW: If direct joining would replace adhesives, it would mean re-planning our production lines. Manufacturing chains could be shortened and combined because the components can be manufactured, joined and further processed in-line.

LIA: What further research is needed in this area?

DW: Fully describing the interdependencies in the boundary layer of the metal-polymer joint exclusively with experimental research will be difficult. For this reason, we are currently working on a multiscale simulation approach to gain better understanding of the interdependencies. One main challenge is to transfer the effects of different surface characteristics (microscale) to strength predictions at component level (macroscale).

LIA: What could this research mean for the future?

DW: Direct joining in general allows redesigning joints in comparison to adhesive bonds. If, in addition, the capability of the joint can be predicted, manufacturing processes can be optimized and the confidence in those joints will be increased.

Photo of Dominic Woitun, Bosch

See Dominic present, “Precise Laser Structures as a Tool to Understand Metal-Polymer Joints“  (Authors: Dominic Woitun, Michael Roderus, Thilo Bein, Elmar Kroner) at the Laser Macroprocessing Conference Track on October 8, 2019. Register for ICALEO here: www.lia.org/conferences/icaleo

SOURCE: https://issuu.com/marketlia/docs/lia_today_augsept-2019/18?fr=sOTg0ZjIzMzQwOA

Surface Functionalization with LIPSS Continues to Expand into New Industries

Interview by Liliana Caldero
As featured in LIA TODAY July/August 2019.

 

Laser researchers from Bundesanstalt für Materialforschung und -prüfung (BAM) have teamed up with medical researchers from Johannes Kepler Universität Linz (JKU) and Kepler Universitätsklinikum Linz (KUK) in a European research project to show the potential of laser materials processing for suppressing the adhesion of human cells to titanium alloy implants such as miniature pacemakers. This is only one of many research projects investigating the potential uses of surface functionalization. With the use of lasers, technical surfaces can be structured at nano- and micro-scales to mimic textures found in nature, copying the unique characteristics that make them hydrophobic, anti-bacterial, or anti-reflective; this is known as surface functionalization. In most cases, this type of processing reduces or even removes the need for certain chemical coatings.

The field of laser-based surface functionalization is expanding rapidly and new potential applications abound; this technology offers innovative solutions for biotechnology, automotive manufacturing, and machine building. As with most new solutions, the big question is how to make it fast and scalable to promote industry-wide adoption

According to Camilo Florian-Baron of BAM, the trick is using linearly polarized high-intensity ultrashort laser pulses to create laser-induced periodic surface structures, or LIPSS, which can produce these desirable biomimetic properties. With advancements in fast laser scanning heads and recent high-repetition rate ultra-short pulsed femtosecond lasers, surface functionalization with LIPSS is becoming more available for R&D and manufacturing. Florian-Baron and his research team are investigating the future of LIPSS applications. With more than 50 publications on LIPSS coming from BAM in the past decade, the group is among the leading institutions progressing the understanding of the interaction between ultrashort laser pulses and matter for micro- and nano-fabrication of materials[1]. Florian-Baron will be presenting at ICALEO 2019 on the latest applications of surface functionalization through LIPSS. He shared with LIA about some of the unexplored potential of this emerging field and some of the interesting projects his team has been honored to work on.

CFB: Usually, materials processing at industrial scales with lasers requires the scanning of the sample of interest with tightly focused laser beams or sweeping the beam on a static sample surface. It means that the micro- and nanofabrication over large areas could take a long time due to the need of irradiating line-by-line or spot-by-spot until the desired machining process is completed. In contrast, laser-induced periodic surface structures (LIPSS) can be fabricated on virtually any material when irradiated with linearly polarized high-intensity ultrashort laser pulses, typically under loosely focusing conditions (large beam spots). The morphology of LIPSS corresponds to parallel arranged period lines featuring periods that can be controlled between only ~100 nm and a few micrometers. Their orientation is strongly influenced by the laser beam polarization used. It means that it is possible, for example, to produce nanometric spaced lines all perpendicular to the laser polarization with a laser beam size at the irradiated surface that is 1000 times bigger than their periodicity covering a larger area with nanostructures faster than conventional laser-direct writing. In an additive approach, these surface nanostructures can be easily superimposed to other surface microstructures, resulting in hybrid surface structures with multiscale surface roughnesses. Through all these surface topographies, along with accompanying laser-induced chemical alterations at the surface, different surface functionalizations can be realized, ranging from structural colorization or antireflective properties (as on certain butterflies), over a control of surface hydrophilicity/-phobicity (as on lotus leaves), and toward unidirectional liquid transport (as realized by moisture-harvesting lizards or bark bugs).

Techniques based on lasers could be defined as contactless digital manufacturing techniques, currently constituting a real industrial- revolution that is transforming the production processes from the early stages of research and development to mass production and marketing [2]. The biggest difference in comparison with other fabrication methods is the possibility to perform design changes using only mouse clicks instead of modifying an already fabricated prototype, resulting in a faster, cheaper and more efficient way of materials processing. Besides that, the current advancements in fast laser scanning heads, combined with high-repetition rate femtosecond lasers allow producing LIPSS at industrially relevant scales and processing speeds, which in the end will be translated into cheaper fabrication costs at higher production rates. Importantly, the whole fabrication process is compatible and reproducible at room temperature and air atmosphere, which is very attractive to most industries that work under similar conditions.

LIA: Your research team has been investigating the mechanisms responsible for the formation of LIPSS to better understand how and when those structures can be formed; what are some of the exciting applications you are researching?

CFB: Our research group is specialized in developing strategies based on lasers to understand the mechanisms of interaction between ultrashort laser pulses and matter, to micro- and nanofabricate materials for specific applications.

Last year, we successfully finished a 3-year international research project funded by the European Commission called LiNaBioFluid [3] where one of the goals was to produce LIPSS on industrially relevant materials and scales to decrease the friction coefficient in tribological applications, as well as developing strategies based on LIPSS for passive fluid transport applications, including commercial lubricants, all based in biomimicking structures found in nature.

As a continuation of this project, currently we are working in another European project called CellFreeImplant [4] (see the link below) that uses LIPSS to avoid unwanted cell growth on medical devices, such as smart medical implants. The promising results are at present in the hands of our medical project partners with close collaborations with a large pacemaker manufacturer to potentially take this laser-based approach for so-called ‘leadless’ pacemakers to real patients in the future.

One of the most exciting feelings when researching LIPSS is that the variety of the current applications are spread over different technological areas. On one hand, this allows us to learn more

Image: Steel sample processed by a femtosecond laser. The colour effects of the four fields result from the diffraction of the ambient light by the laser-induced periodic nanostructures on the surface. Source: BAM, Division Nanomaterial Technologies

about the real producer and manufacturer problems, while at the same time solving them in an efficient way. On the other hand, and personally, with the research that we are currently doing at

BAM, I feel that I am not only achieving milestones in a research project to fulfill it, I think that one day the research, time and resources we are investing could be applied in this particular case to real medical devices that any person can benefit from. In the end, the feeling is that with our tiny steps, we are making the world a better place.

 

LIA: With all that is being done already, what additional research would you like to see happen in this field?

CFB: Currently, the understanding of the formation dynamics achieved by the growing community of scientists researching LIPSS have allowed the development of different applications in different and diverse fields. However, due to the many different and specific conditions needed to fabricate them, a general model that includes all the possible experimental outcomes in the different materials is not available yet. More efforts should be focused on developing more complete models that will provide a deeper understanding of the formation mechanisms and

laser-matter interaction dynamics that give rise to LIPSS structures. Consequently, with more understanding of the mechanisms involved, novel and innovative applications could emerge.

There are several areas where LIPSS could be useful but currently are barely explored, such as the case of catalytic and self-cleaning surfaces, antireflective treatments based on nanostructures instead of organic or inorganic coatings and perhaps bacterial or antibacterial surfaces for food manufacturing or applications in medicine [1,4,5].

From a practical point of view, the production speed of LIPSS is currently further boosted up by several research groups in Germany, France and Spain, featuring novel scanner technologies based on polygon scanners, along with high repetition rate ultrashort laser sources reaching MHz to GHz pulse repetition rates.

References

  1. http://doi.org/10.1109/JSTQE.2016.2614183 : Laser-induced Periodic Surface Structures – A Scientific Evergreen (Open access)
  2. https://www.tdx.cat/bitstream/10803/400403/1/CFB_THESIS.pdf
  3. https://www.bam.de/Content/EN/Standard-Articles/Topics/Energy/article-linabiofluid.html
  4. https://www.researchgate.net/project/CellFreeImplant-Cell-free-Ti-based-Medical-Implants-due-to-Laser-induced-Microstructures-H2020-FETOPEN-4-2016-2017-CSA.
  5. https://doi.org/10.1007/s00339-017-1352-0 (Open access)
  6. https://doi.org/10.1016/j.apsusc.2017.02.174

 

Photo of Camilo Florian-Baron, Bundesanstalt für Materialforschung und -prüfung (BAM)

See Camilo present, “Surface Functionalization by Laser-Induced Periodic Surface Structures“  (Authors: Camilo Florian-Baron, Sabrina V. Kirner, örg Krüger, Jörn Bonse) at the Laser Nanomanufacturing Conference Track on October 8, 2019. Register for ICALEO here: www.lia.org/conferences/icaleo

 

SOURCE:  https://issuu.com/marketlia/docs/lia_today_augsept-2019/10?fr=sZjFhZTIzMzQwNg

Killing Cancer at the Speed of Light

As featured in LIA TODAY

By Liliana Caldero

 

LITT
Brain cancers make up about 1.4% of all new cancer cases in the U.S. (NCI, 2018). Surgery is an important part of managing these cancers, with the goal of removing the tumor when possible. Doing this safely can present a challenge when the tumor is located in critical areas of the brain such as the brainstem, basal ganglia, or thalamus. This is where Laser Interstitial Thermal Therapy, or LITT, is offering hope to patients.

According to Dr. Arnold B. Etame, a Neurological Surgeon and Scientist at Moffitt Cancer Center, Magnetic Resonance Imaging (MRI) guided LITT is being used to treat brain tumors that were once considered inoperable with traditional surgery due to their location. LITT can be used to destroy tumors in critical areas, while minimizing the potential for damaging healthy brain tissue and also offering an incredibly short recovery time.

 

HOW IT WORKS
Using highly advanced MRI-guidance technology, the surgeon identifies critical areas of the brain in relation to the tumor, and then maps out the entryway and target. A very small incision, about 3-4 mm wide, is made at the entryway, and a laser fiber probe is inserted and guided into the target. New technology allows the MRI to occur at the same time, providing the guidance needed for precision during the procedure. From behind a protective barrier, the surgeon operates the laser remotely while monitoring the patient. Using pulsed laser energy, the tissue of the tumor is ablated, or burned away, while the surrounding healthy brain tissue remains.

As incredible as this treatment approach is, Etame is sure to point out that LITT is only one of many important techniques used in the treatment of brain cancers, and that there are many situations in which traditional surgery would be effective based on the treatment goals. “Traditional approaches have come a long way – we use MRI-guided functional mapping for language or movement, we also use tractography to look at white matter fibers in relation to the tumors, as well as keep patients awake during procedures to monitor their functioning. The laser is reserved for more challenging situations.” Situations like radiation necrosis.

“It’s a new technique,” says Etame, “which over the past few years has been shown to have some utility in specific cases. These scenarios include tumors or lesions in difficult-to-reach areas of the brain, tumors near critical structures where precise targeting is required, radiation irritation of the brain (this is known as radiation necrosis), or recurrent aggressive tumors that progress despite prior surgery and radiation.” Etame also refers to several studies in which LITT has been effective with recurrent gliomas and glioblastomas in challenging locations such as the Thalamus. He explains that when compared with standard craniotomies for resection of brain tumors, the recovery time after LITT is significantly quicker, and there are significantly fewer complications. “Patients can resume other important cancer therapies, such as chemotherapy and radiotherapy, very quickly.”

 

THE NEED FOR RESEARCH
Continued research is shedding light on the other potential applications of LITT. “One area where it has been applied heavily,” Etame says, “has been the destruction of seizure causing tissue. When an area of the brain that causes the epileptic seizures can be identified, removal or destruction of that area with the laser can help with seizure control. This is currently used a lot for epilepsy of the temporal lobe in children, as well as in some adults.”

Moffitt Cancer Center is one of the few facilities in the U.S. currently utilizing LITT. “Not every center has the technology; that in itself could be a limitation,” says Etame. “For certain things, traditional surgery can be used as an alternative to [LITT] and surgeons may use a technique based on their comfort level with that technique.” So what would it take for more facilities to adopt LITT as a treatment modality? “I think what is important is conduction of large prospective studies to better understand which tumor pathologies are much more amenable to the long-term benefits of laser ablation, which will improve patient selection.”

Like other treatments, LITT is only as effective as the selection of the patient and the tumor. For example, there are situations where a tumor is highly vascular, meaning that a lot of blood is flowing to it. This essentially turns it into a heat sink, which would make LITT ineffective. There are also situations in which a biopsy of the tumor tissue is needed to identify which treatments the cancer will respond to best. In that case, destroying the tissue with the laser would cause the loss of valuable information, although Etame notes that it is possible to perform a biopsy first and then ablate the tumor after, if the situation calls for it.

Lasers continue to be a valuable tool in modern medicine, and thanks to ongoing research we are seeing new biomedical applications with the potential to save lives.

 

Learn More

National Cancer Institute
https://www.cancer.gov/

Moffit Cancer Center
https://moffitt.org/cancers/brain-cancer/your-brain-tumor-specialists/

LITT for Epilepsy
https://www.epilepsy.com/learn/professionals/diagnosis-treatment/magnetic-resonance-guided-laser-interstitial-thermal-therapy

Laser Additive Manufacturing’s Journey to Commercialization

By Andrew Albritton

As seen in LIA TODAY

LASER ADDITIVE MANUFACTURING CHALLENGES

Laser Additive Manufacturing (LAM), as it pertains to powder based manufacturing, is a technique that utilizes the interaction of lasers and base materials to construct a product, rather than removing material from a pre-constructed block of material. LAM is quickly approaching the critical point of being more than a method to produce prototypes and small runs of one-off parts – it is poised to turn everything we know about mass production on its head. Professor Dr. Minlin Zhong, President-Elect of LIA and Director of the Laser Materials Processing Research Center at Tsinghua University, believes it surpasses all available alternative methods.  Prof. Dr. Zhong  says “LAM shows obvious advantages on freeform manufacturing, including free geometry, free structures, free strengthening mechanism, free microstructures, free performance and even free scale (from macro, to meso, to micro, to nano),”. Manufacturers who use LAM are able to reduce the waste of materials commonly associated with traditional subtractive manufacturing methods; decrease the weight of parts by cutting out filler materials; and have more control over material properties resulting in stronger, more complex, lighter, and more efficient parts. With such exceptional technology currently at our disposal, why hasn’t LAM been more widely adopted?

IT’S EXPENSIVE

One of the most commonly cited reasons is that the costs to produce parts through LAM are prohibitive. The key driver of these high costs is that the supply chain for metal powders is not yet optimized for LAM technology. Materials are expensive, custom made, or not readily available. The Metal Powder Industries Federation (MPIF) states in its 2017 PM Industry Roadmap that, “A better understanding of the precursor materials impact on the metal AM process is required. Traditionally, precursor materials have been existing thermal spray powders that have not been refined/tuned to the AM process limiting optimization.” LAM parts producers are often using metal powders that have not been designed for use in LAM processes, which frequently results in suboptimal products.

According to MPIF, as of 2017, there are approximately 12 suppliers of metals for Additive Manufacturing (AM) for the international market, most produce stainless steel, cobalt-chrome, and titanium, with a few supplying aluminum alloys, copper, super alloys, platinum, Inconel, tungsten, molybdenum, and tool steels. With so few suppliers and a sparse number of common material types, there is a bottleneck for providing quality affordable metal powders to the LAM industry. With companies expanding the selection of materials that can be laser processed, it is vital that the problem of material availability be resolved. For example, Nuburu has produced a “blue” laser which operates at the 450 nm wavelength, and is capable of processing gold, aluminum, brass, and copper.

SUPPLY AND DEMAND

What can be done to improve the supply chain and reduce the cost of LAM part production? The metal powder industry does not supply enough quality powder to support widespread adoption of LAM, while early adopters of LAM applications do not create enough demand to drive competition into the metal powder market to reduce prices. A first step to get these industries operating in unison will be the creation and mass adoption of standards, specifications, and best practices in regards to metal powders. By standardizing metal powder properties for best final product properties, metal powder suppliers would be able to build up an inventory without relying on custom special orders. Specifications on how surplus powder from a project can be reused could also help introduce addition cost savings to manufacturers.

STANDARDS FOR QUALITY CONTROL

Another hurdle for LAM is microstructural quality, uniformity, and repeatability. To become a replacement for more legacy manufacturing methods, LAM needs to produce parts consistently and continuously that are to specifications. With traditional subtractive manufacturing methods, there are several quality control points where product is inspected and defects are addressed prior to the next step, resulting in no wasted effort past the point of failure. With LAM, the part in question is created from the ground up; this determines the final product’s quality, microstructure, and mechanical properties simultaneously. The process is completed with either a perfect or defective final product. Paul Denney, Director of Advanced Process Development with IPG Photonics, states, “Unlike machining where you start with a “block” of material with known quality and properties, additive production of parts requires a combination of motion with the prediction of the microstructures, mechanical properties, and stresses. Because the properties are closely connected to how the material is deposited, this greatly complicates the development of processing procedures and parameters.”

What methods can be implemented into a given LAM process to help ensure quality of the final product? The first quality control concerns are addressed long before the process begins. Starting materials must be certified as appropriate for the application, the order of operations of the production device should be scrutinized to ensure that the final product will be to spec with minimal waste, and the machine itself must be operating at peak parameters. As the production of a LAM product can take an extended amount of time, any loss of power to the point of interaction can have detrimental effects to the end product and even the products in queue. Loss of power can be caused by an actual power failure, a dirty or damaged optic, or other origins. With the structural integrity of a LAM part resting critically on the success of every step of the process, it is imperative that the process is stringently optimized and the machine is operating at peak performance. Here is what Paul Denney has to say about the subject:

“Because of the additive manufacturing approach in bed based systems, even if defects can be detected and possibly ‘corrected’, any changes may not be possible. An example of this may be what is done if a ‘defect’ is flagged in a single part in a batch of parts being produced. One approach would be to stop the processing and ‘correct’ the defect. However, if this is done then the thermal history for all of the parts may be altered and all parts may now be out of the desired properties. Another approach would be to stop processing on the part with the defect, but this again would alter the heat load on the complete batch or the time between other parts being produced which may again alter the properties. So any monitoring system will need to detect changes prior to the formation of any defects while at the same time any corrections must be made within the acceptable parameter range.”

There is a thin line between success and failure: one small interruption can ruin an entire batch of product. What can be done to prevent this?

As Paul explained, this is not a single issue, LAM processes need both a method to detect defects and the ability to immediately respond to them. A starting point is to ensure that redundancies are incorporated into the build process so that if a common defect occurs at a certain stage, there are defined responses the system can take automatically to correct them. In the case of a laser lens issue, it may be beneficial to incorporate additional laser delivery systems to the process as a redundancy to pick up where a suboptimal device has failed in real time.

EVALUATING THE FINAL PRODUCT

In addition to inline defect detection, the industry as a whole will require a standardized best practice for evaluating finalized parts. For traditional manufacturing methods, a sample of the produced part pool is selected for evaluation via destructive and non-destructive tests to certify whether a set of parts are built to specifications. As many LAM-produced parts are complex and costly to produce, it seems wasteful to destroy a set of them to certify them. In the paper “Evaluation of 3d-Printed Parts by Means of High-Performance Computer Tomography” presented at ICALEO 2017, authors Lopez, Felgueiras, Grunert, Brückner, Riede, Seidel, Marquardt, Leyens, and Beyer reviewed the viability of X-ray Computer Tomography (CT) and 3d scanning as methods to detect inferior AM parts. The paper concludes that the CT method best fits the needs of the AM industry. According to Lopez et. al, “Computer tomography can quantify all complex structures in scope of the proposed demonstrator and delivered deviation values of the measured structure, providing a good base for comparison across demonstrators made by different methods, materials and dimensions. Porosity or defects down to 3 µm can be determined by the used CT system.” Currently, CT scanning a LAM part is a time consuming process, but with additional focus on improvement it could become an essential quality non-destructive control method for finalized parts to evaluate complex internal structures.

TOO MANY ALTERNATIVES

A third barrier to the spread of LAM is the multitude of alternative methods in the industry. As stated by Prof. Dr. Zhong, “Some conventional metal deposition technologies such as arc building-up welding, plasma building-up welding and electronic building-up welding can also fabricate metallic components in near shape. Their deposition rate and productivity may be high and the costs may be lower, but normally they are limited in fabricating complex geometry and accuracy.” Freeform manufacturing is where LAM excels, but despite its many advantages over alternative methods, it has an Achilles heel.

One advantage of alternative manufacturing methods is the speed at which a product can be produced. However, according to Paul Denney, this speed gap is closing faster every day.

“While higher laser powers allow for higher deposition rates but at the expense of lower resolution, some researchers are looking to maintain the resolution by combining multiple lasers into an additive deposition system. Research groups and equipment builders are investigating how best to handle multiple lasers in the same processing area. There are other areas that may be investigated including power distribution to improve the interaction between the power and laser beam to improve efficiency of the process and to minimize defects. This could improve the deposition rates while at the same time maintaining quality.”

Prof. Dr. Zhong hopes that soon LAM researchers will, “improve the materials diversity, increase the dimension (to square meters), increase the deposition rate and decrease costs. A hybrid approach to combine LAM with the conventional additive manufacturing methods may be a solution to achieve the above targets.” The concept of a hybrid production system that can combine multiple lasers with fast alternative methods where complexity is not a requirement could lend itself to faster build times.

THE LATE ADOPTERS

Earlier in the article, we touched on the final barrier to the wide spread success of LAM: industry standards. Current standard offerings from ASTM and ISO cover Design, Materials and Processes, Terminology, and Test Methods. Additionally, new processes are created frequently and new standards are being developed every year in an attempt to keep up. It is unclear how much of the industry has adopted these existing specifications. Until the entire market accepts a set of standards for all steps of the Additive Manufacturing process and supply chain, the evaluation of AM parts will remain a costly endeavor that will limit AM’s potential. MPIF expresses a bleak outlook on metal AM in its State of the PM Industry in North America – 2017 document: “Despite all the fanfare, true commercial long-run production still revolves around only three product classes: titanium medical implants, cobalt-chrome dental copings, and cobalt-chrome aircraft nozzles.” The truth of the matter remains that without a set of clearly defined standards, the LAM industry will continue to remain confined to early adopters like the Aerospace and Medical fields. With the benefits in intricacy and weight saving advantages LAM should have obvious opportunities in the automotive and electronics industries.

Markets are watching LAM for innovative uses before taking the plunge and embracing the technology. Currently, LAM may appear to have a bad Return on Investment (ROI) if producers only hope to replicate their existing products through LAM rather than innovating their parts to capitalize on its strengths. In the words of Paul Denney, “If AM is supposed to make big impact, companies are going to have to rethink their parts; determine how AM allows for changes in the design and possibly improve the performance. The benefits can come in many forms which could be a weight savings, a production savings, and/or a performance savings.” The industry needs to challenge its way of thinking about production to allow the benefits inherent to LAM to propel their production and parts to new levels of performance. Paul Denney provided the following illustration: “With the formation of properties ‘locally’ instead of in ‘bulk,’ it is possible to produce ‘gradient’ materials. The ‘gradient’ can come by changes to the properties of a given chemistry of material or by using materials with different chemistries. As an example: a bracket could be produced for a jet engine that has high temperature properties near the engine but as the bracket extends to an attachment point, the properties/chemistry can be altered to improve the fatigue properties.”

LAM has a bright future and many engineers and scientists are working to unlock its full potential. Once the barriers of the supply chain, dynamic quality control, speed of production, and process standardization have been resolved, it is highly likely the LAM will be a manufacturing method of choice.

 

ACKNOWLEDGEMENTS

Paul Denney, Director of Advanced Process Development with IPG Photonics and LIA’s Past President

Prof. Dr. Minlin Zhong, Director of Laser Materials Processing Research Center at Tsinghua University

and LIA’s President-Elect

 

References:

Lopez, E., Felgueiras, T., Grunert, C., Brückner, F., Riede, M., Seidel, A., Marquardt, A., Leyens, C., Beyer, E. (2018). Evaluation of 3D-printed parts by means of high-performance computer tomography. Journal of Laser Applications 30, 032307; https://doi.org/10.2351/1.5040644